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The book“A manual of Physical Chemistry Practicals with viva questions" volume 1, (Basic) For B.Sc. and M.Sc. chemistry students is designed for B.Sc. and M.Sc. chemistry students of Indian Universities. The salient point of the book is the inclusion of viva questions with answers with explanations at the end of each chapter. The list of experiments assembled here will be useful for B.Sc. and M.Sc. chemistry students. To make the students understand better, attempts have been made to explain the mechanism behind all the experiments in the principle section. The author has teaching and research experience in physical chemistry of more than three decades. The book has been written keeping in view the needs of the students.